KWS-3 'VerySANS'

focusing VSANS diffractometer operated by JCNS@MLZ

User Tools

Site Tools

kws-3

KWS-3 'VerySANS'

unofficial page of focusing VSANS diffractometer operated by JCNS@MLZ

  • KWS-3 is a very small angle neutron scattering (VSANS) diffractometer operated by JCNS at Heinz Maier-Leibnitz Zentrum (MLZ) in Garching, Germany.
  • KWS-3 is historical official name of the instrument. JCNS at MLZ is operating two more KWS-x instruments: two classical pinhole SANS diffractometers KWS-1 and KWS-2. To show that KWS-3 differs from pinhole SANS instruments, KWS-3 obtained the second name 'VerySANS'.
  • The principle of this instrument is one-to-one imaging of an entrance aperture onto a 2D position sensitive detector by neutron reflection from a double-focusing toroidal mirror.
  • In current state [2021], KWS-3 is covering Q-range between 3·10-5 and 3·10-1 Å-1 and used for the analysis of structures between 20 Å and 20 μm for numerous materials from physics, chemistry, materials science and life science, such as alloys, diluted chemical solutions, hydrogels and membrane systems.
  • Within the last few years we have finalized several big “evolutionary” projects; we have completely re-designed and commissioned the main components of the instrument: selector area, mirror positioning system, main sample station at 10m, beam-stop system; implemented new sample stations at 3.5 and 1.3m, second (very-high resolution) detector, polarization and polarization analysis systems; adapted the instrument to almost any existing/requested sample environment like 6-position Peltier furnace (-25°C to 140°C), high-temperature furnace (< 1600°C), cryostats/inserts (>20 mK), liquid pressure cell (<5 kBar/10-80°C), CO2/CD4 gas pressure cell (<0.5 kBar/10-80°C), humidity cell/generator (5-95%/10-90°C), magnets (horizontal < 3T, vertical < 2.2T), Bio-logic® multimixer stopped flow (5-80°C), rheometer RSA II (tangential/radial) etc.



Focusing Element:

Toroidal Mirror

  • Geometry of the instrument is defined by geometry of the mirror
  • Shape: Toroidal ≈ Ellipsoidal
  • Size: 120x12x8cm3 (2x 60x12x8cm3)
  • Toroid: RadiusMeridional=531m; RadiusSagittal=0.224m
  • Focus-to-Focus Distance: 22m
  • Ellipse semi-axises: 11.230m and 0.224m
  • Coating 65Cu: m=1, λ=12.8Å ⇒ θc=0.1·m·λ=1.28°
  • λ=12.8Å: θ=[1.16°… 1.23°]

Highest Resolution

(V)SANS instrument  Beam image in the highest resolution configuration

  • High Brilliance Neutron Source
  • 2D Focusing Toroidal Mirror
  • Non-magnetic coating 65Cu
  • Ångstrom roughness ⇒⇓
  • Signal-to-noise ratio: better 105
  • Geometrical focusing, λ independent
  • ~ 100% reflectivity above 12Å [10Å:<10% and 8Å: <1%]
  • Q-range: 3·10-5 … 3·10-1 Å-1
  • Best resolution: 3·10-5Å-1 ⇒ 20μm
  • Lowest resolution: 3·10-1Å-1 ⇒ 20Å
  • Broad Dynamical Range: Qmax/Qmin=104


Mirror & detector are movable

Modes: (V)SANS, GiSANS, Reflectometry



Flux vs. Sample-to-detector distance

  • Flux at the detector: ≈ 6000 n/sec/mm2 [12.8Å]
  • Flux at the sample: ∼D2
  • Maximal beam size at the sample is defined by the mirror geometry

                ≈ 80x20mm2 at SDD≈10m

                ≈ 35x10mm2 at SDD≈4m

                ≈ 10x 5mm2 at SDD≈1.6m



Status 2020

  • Sample-to-detector distance: 10m, 9.5m, 1.3m (User Mode) and 0.03 to 0.45m (Test Mode)
  • Wide Q-range: 4·10−5 < Q <2.5·10−2 Å−1 (9.5m & 1.3m, λ=12.8Å, VHRD & HRD)
  • Qmin =2·10−5 Å−1 (#0 SD=10m, λ=30Å)
  • Qmax = 0.45 Å−1 (#4 SD=0.05m, λ=12.8Å)



Status 2022: multi sample position approach



Q-range: compact sample environment

9.2m, 1.6m, 0.3m and 0.05m



Q-range: bulky sample environment

10m, 4m, 3m and 2m

kws-3.txt · Last modified: 2022/09/25 05:46 by Vitaliy Pipich